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Wood Science and Technology

11.04.2024 | Original

Aqueous modification of waterlogged archaeological wood by phenylboronic acid to reduce hygroscopicity and improve the dimensional stability

verfasst von: Yihang Zhou, Yue Zhang, Liyan Kan, Yue Wang, Kai Wang, Dongbo Hu

Erschienen in: Wood Science and Technology

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Abstract

During the dehydration of waterlogged archaeological wood (WAW), shrinkage inevitably occurs due to capillary force and hydrogen bond recombination as WAW loses free and adsorbed water. Existing drying techniques, including solvent displacement, freeze-drying, and supercritical fluid drying, only take effect by reducing or eliminating the surface tension of liquid. Nonetheless, the contribution of hydrogen bond recombination in shrinkage has long been neglected and a countermeasure concerning this problem is needed. In this study, we propose a simple aqueous phenylboronic acid (PBA) treatment that can help improve dimensional stability and reduce hygroscopicity of WAW. Analysis by Fourier transform infrared spectroscopy, density functional theory calculation and dynamic vapour sorption reveal that PBA can incorporate with hydroxyl groups (–OH) on cellulose through coordination and hydrogen bonds, occupy the water-cellulose binding sites, and possibly inhibit the formation of hydrogen bonds between adjacent cellulose chains.

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Titel: Aqueous modification of waterlogged archaeological wood by phenylboronic acid to reduce hygroscopicity and improve the dimensional stability
verfasst von: Yihang Zhou
Yue Zhang
Liyan Kan
Yue Wang
Kai Wang
Dongbo Hu
Publikationsdatum: 11.04.2024
Verlag: Springer Berlin Heidelberg
Erschienen in: Wood Science and Technology
Print ISSN: 0043-7719
Elektronische ISSN: 1432-5225
DOI: https://doi.org/10.1007/s00226-024-01551-4