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European Journal of Wood and Wood Products

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03.12.2022 | Original Article

Moisture desorption isotherms and thermodynamic properties of two dense tropical woods: Tali (Erythrophleum suaveolens Brenan) and Bilinga (Nauclea diderrichii Merr)

verfasst von: Banyuy Godwin Fonyuy, Jean Gaston Tamba, Joseph Zobo Mfomo, Armand Fopah-Lele, Benjamin Salomon Diboma, Dominique Martial Manga Bengono, Evariste Fongnzossie Fedoung, Achille Bernard Biwolé

Erschienen in: European Journal of Wood and Wood Products | Ausgabe 3/2023

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Abstract

The aim of this study was to determine moisture desorption isotherms and some thermodynamic properties of two dense tropical woods from Cameroon: Tali (Erythrophleum suaveolens) and Bilinga (Nauclea diderrichii), which are classified as medium-heavy (Bilinga) and heavy (Tali) woods with high economic values. Equilibrium moisture contents (EMC) were determined using the static gravimetric method at three temperatures (30 °C, 40 °C, 60 °C) and relative humidities (RH) between 5.5 and 83.6%. For thermodynamic properties, Gibbs free energy (GFE), net isosteric heat (q_st,n) and differential entropy (ΔS) were determined using Clausius Clapeyron and Avramidis equations. To interpret hygroscopic behavior and thermodynamic properties, anatomical and chemical structures were analyzed using microscopic images and infrared (IR) spectroscopy respectively. EMC decreased from 19.39 to 1.99% for Bilinga and from 11.17 to 0.51% for Tali as temperature increased. GAB model best described desorption isotherms data. Desorption isotherms recorded type II sigmoids. Anatomical analysis revealed that Tali and Bilinga had porosities of 40.52 and 50.32%, 3–6 and 6–12 vessels/mm², 400–700 µm and 700–1000 µm rays respectively. Specific Surface Areas (SSA) decreased from 155.602 to 57.115 m²/g for Tali and 287.692 to 175.688 m²/g for Bilinga. This result supports the isotherms measurement in terms of hygroscopic capacity of woods. Positive thermodynamic properties revealed that desorption was non-spontaneous and the difference between harmonic mean and isokinetic temperatures confirms an enthalpy-entropy compensation theory. q_st,n is higher for Tali implying it is less hygroscopic and requires more energy than Bilinga.

Vorheriger Artikel Effects of acetylation on moisture sorption of wood under cyclically changing conditions of relative humidity

Nächster Artikel Essential oils from Thymus spp. as natural biocide against common brown- and white-rot fungi in degradation of wood products: antifungal activity evaluation by in vitro and FTIR analysis

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Titel: Moisture desorption isotherms and thermodynamic properties of two dense tropical woods: Tali (Erythrophleum suaveolens Brenan) and Bilinga (Nauclea diderrichii Merr)
verfasst von: Banyuy Godwin Fonyuy
Jean Gaston Tamba
Joseph Zobo Mfomo
Armand Fopah-Lele
Benjamin Salomon Diboma
Dominique Martial Manga Bengono
Evariste Fongnzossie Fedoung
Achille Bernard Biwolé
Publikationsdatum: 03.12.2022
Verlag: Springer Berlin Heidelberg
Erschienen in: European Journal of Wood and Wood Products / Ausgabe 3/2023
Print ISSN: 0018-3768
Elektronische ISSN: 1436-736X
DOI: https://doi.org/10.1007/s00107-022-01907-2

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